- Efficient and recyclable catalyst of palladium nanoparticles stabilized by polymer micelles soluble in water for Suzuki-Miyaura reaction, Ostwald ripening process with palladium nanoparticles.
[作者:Beletskaya, Irina P.;Kashin, Alexander N.;Khotina, Irina A.;Khokhlov, Alexey R.;,期刊:SYNLETT, 页码:1547-1552 , 文章类型: 研究论文,,卷期:2008年-10]
- The Suzuki-Miyaura cross-coupling reaction of aryl iodides and bromides with areneboronates, catalyzed by Pd-contg. water-sol. micelles formed by PS-PEO copolymer and N-cetylpyridinium chloride as a surfactant, was studi...
- Facile and selective synthesis of propargylic amines and 1,6-diynes: one-pot three-component coupling reactions of alkynylsilanes, aldehydes and amines by a cooperative catalytic system comprised of CuCl and Cu(OTf)2.
[作者:Sakai, Norio;Uchida, Naoki;Konakahara, Takeo;,期刊:SYNLETT, 页码:1515-1519 , 文章类型: 研究论文,,卷期:2008年-10]
- Described herein is a three-component coupling reaction of alkynylsilanes, aldehydes, and amines by a cooperative catalytic system comprised of CuCl and Cu(OTf)2, leading to the prodn. of a variety of propargyl amine der...
- Efficient synthesis of (3R,5S)-3,5,6-trihydroxyhexanoic acid derivative as a chiral side chain of statins.
[作者:Choi, Hyeong-wook;Shin, Hyunik;,期刊:SYNLETT, 页码:1523-1525 , 文章类型: 研究论文,,卷期:2008年-10]
- Efficient synthesis of (3R,5S)-6-hydroxymethyl-2,2-dimethyl-1,3-dioxane-4-acetate (I) was accomplished. Unprecedented hydration of (S)-4-hydroxyfuran-2-ylideneacetate in the presence of LiCl provided (R)-5,6-dihydroxy-3...
- Expedient Mukaiyama-type Mannich reaction catalyzed by lithium chloride.
[作者:Hagiwara, Hisahiro;Iijima, Daiki;Awen, Bahlul Z. S.;Hoshi, Takashi;Suzuki, Toshio;,期刊:SYNLETT, 页码:1520-1522 , 文章类型: 研究论文,,卷期:2008年-10]
- The Mannich reaction of methylsilyl enol ether with aryl aldimine proceeded in the presence of a catalytic amt. of LiCl in DMF at room temp. The reaction was mild enough to apply to aldimines having the AcO, Me3CMe2SiO,...
- A simple zinc-mediated preparation of selenols.
[作者:Santi, Claudio;Santoro, Stefano;Testaferri, Lorenzo;Tiecco, Marcello;,期刊:SYNLETT, 页码:1471-1474 , 文章类型: 研究论文,,卷期:2008年-10]
- Under acidic conditions zinc reduces diselenides to afford selenols, which can be either isolated or treated in situ with alkyl halides to produce alkyl selenides or with epoxides to give b-hydroxyselenides.
- Synthesis of 8-heteroaryl-2'-deoxyguanosine derivatives.
[作者:Hobley, Gerard;Gubala, Vladimir;Rivera-Sanchez, Maria Del C.;Rivera, Jose M.;,期刊:SYNLETT, 页码:1510-1514 , 文章类型: 研究论文,,卷期:2008年-10]
- We describe the synthesis of 8-hetaryl-2'-deoxyguanosine analogs using Suzuki-Miyaura or Stille conditions. Unprotected and protected 8-bromo-2'-deoxyguanosine was coupled with com. available hetarylboronates or trialky...
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