One-Pot Synthesis of Ammonia-Borane and Trialkylamine-Boranes from Trimethyl Borate

[摘要]：A one-pot procedure for the preparation of ammonia borane from trimethyl borate in 90% yield and >99% purity has been reported. This methodology has been modified to prepare a series of trialkylamine-boranes in 70-82% yields from trimethyl borate and lithium hydride/aluminum chloride in the presence of the corresponding trialkylamine.

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