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[摘要]:Ests. of intramol. distances are essential for structure detn. For medium-sized mols., ROESY NMR spectroscopy is the method of choice for obtaining distances. However, the integration of ROESY cross-peaks is problematic, owing to the offset dependence of the integrals and/or TOCSY artifacts. We here present EASY ROESY (Efficient Adiabatic SYmmetried ROESY), which yields reliable intramol. distances without a sample-specific setup. |
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