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EASY ROESY: reliable cross-peak integration in adiabatic symmetrized ROESY.

  作者 Thiele, Christina M.;Petzold, Katja;Schleucher, Juergen;  
  选自 期刊  Chemistry-A European Journal;  卷期  2009年15-3;  页码  585-588  
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[摘要]Ests. of intramol. distances are essential for structure detn. For medium-sized mols., ROESY NMR spectroscopy is the method of choice for obtaining distances. However, the integration of ROESY cross-peaks is problematic, owing to the offset dependence of the integrals and/or TOCSY artifacts. We here present EASY ROESY (Efficient Adiabatic SYmmetried ROESY), which yields reliable intramol. distances without a sample-specific setup.

 
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