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Silica sulfuric acid-activated poly-1,3-dichloro-5-methyl-5-(4'-vinylphenyl)hydantoin (PDCVH) as an effective reagent for oxidation of 1,3,5-trisubstituted 2-pyrazolines both under microwave irradiation and thermal conditions.

  作者 Azarifar, Davood;Maleki, Behrooz;Setayeshnazar, Mehrnaz;  
  选自 期刊  Heterocycles;  卷期  2008年75-3;  页码  669-673  
  关联知识点  
 

[摘要]Oxidn. of 1,3,5-trisubstituted 4,5-dihydro-1H-pyrazoles to the corresponding pyrazoles has been achieved by utilizing silica sulfuric acid-activated poly-1,3-dichloro-5-methyl-5(4'-vinylphenyl)hydantoin in EtOH under both microwave irradn. and conventional thermal conditions at room temp. with good yields.

 
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