Selective Monolithiation of Dibromobiaryls Using Microflow Systems.

[摘要]：Selective monolithiation of 2,2'-dibromobiphenyl, 4,4'-dibromobiphenyl, 2,7-dibromo-9,9-dioctylfluorene, 2,2'-dibromo-1,1'-binaphthyl, and 5,5'-dibromo-2,2'-bithiophene, with 1 equiv of butyllithium followed by reaction with electrophiles was achieved using a microflow system by virtue of fast micromixing and precise temp. control. Sequential introduction of two different electrophiles based on this method was also achieved using a microflow system composed of four micromixers and four microtube reactors.

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