One-Pot Catalyst-Free Synthesis of beta- and gamma-Hydroxy Sulfides Using Diaryliodonium Salts and Microwave Irradiation

[摘要]：A simple and rapid one-pot protocol is described for the preparation of alpha- and beta-hydroxy sulfides. The direct solvent-free microwave irradiation of diaryliodonium salts, potassium thiocyanate, and ethylene glycol/beta-propylene glycol without any catalyst or base affords the final compounds in good yields (65-95%) in around 10-25 min.

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