Convenient Preparation of Long-Chain Dialkyl Phosphates: Synthesis of Dialkyl Phosphates

[摘要]：Reaction of phosphorus oxychloride with a primary alcohol (1.8 equiv) and triethylamine (1.8 equiv) in toluene, followed by filtration and treatment with steam, gives dialkyl phosphates in good yield and essentially free from trialkyl phosphate contamination.

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