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[摘要]:Pentafluorinated phenyl-monohydro[60]fullerenes [C-60(Arf)(5)H] are synthesized in good yields via reaction of the corresponding fluorinated phenyl copper reagent, itself prepared in situ from the fluorinated phenyl Grignard reagent (ArfMgBr) and copper(I) bromide-dimethyl sulfide complex, with [60] fullerene (C-60) in 1,2-dichlorobenzene under a nitrogen atmosphere. |
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