【文章名】Facile One-Pot Synthesis of [1,2,4]Triazolo[3,4-b][1,3,4]thiadiazines and 3,7-Dimethyl-4H-[1,2,4]triazino[3,4-b][1,3,4]thiadiazin-6-one Using Heteropolyacid Catalysts
Facile One-Pot Synthesis of [1,2,4]Triazolo[3,4-b][1,3,4]thiadiazines and 3,7-Dimethyl-4H-[1,2,4]triazino[3,4-b][1,3,4]thiadiazin-6-one Using Heteropolyacid Catalysts
作者
MOTAMEDI RADINEH; MONFARED AAZAM; NEZAMABADI ZOHRE GHAHGHAI; BAMOHARRAM FATEMEH F
[摘要]:[1,2,4]Triazolo[3,4-b][1,3,4] thiadiazines 2a-f and 3,7-dimethyl-4H-[1,2,4] triazino[3,4-b][1,3,4]thiadiazin-6-one 4 were synthesized by one-pot cyclocondensation reaction with alpha-chloroacetonitrile and alpha-haloketones in the presence of catalytic amounts of heteropolyacids in very high yields and rates.