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An approach to benzannelated [5,6]-spiroketals.

  作者 Bray, Christopher D.;  
  选自 期刊  SYNLETT;  卷期  2008年-16;  页码  2500-2502  
  关联知识点  
 

[摘要]Heating a variety of 2-hydroxybenzyl acetates bearing a range of functional groups on the 4- or 5-position of the arom. ring at 100?in neat g-methylene-g-butyrolactone (1.0 M) for 20 h gives a series of benzannelated [5,6]-spiroketals in 75-89% yield.

 
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