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THE SYNTHESIS, STRUCTURE AND REACTIVITY OF 1-THIOXOTETRAHYDROPYRIDAZINO[1,2-a][1,2,4]TRIAZIN-4(1H)-ONE

  作者 JARRETT SANDRA; BROWN AINKA; SINGHWILMOT MARVADEEN  
  选自 期刊  Heterocycles;  卷期  2009年78-11;  页码  2755-2768  
  关联知识点  
 

[摘要]The synthesis of 1-thioxotetrahydropyridazino[ 1,2-a][1,2,4]triazin-4(1H)-one 3 in five steps from tert-butyl carbazate and its transformation into 3-benzylidene and 1-amino derivatives are described. Its crystal structure is presented showing it to be an axially chiral molecule that exists as a racemate in the solid state.

 
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