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An Efficient One-Pot Three Component Synthesis of 1,2-Dihydro-1-arylnaphtho[1,2-e][1,3]oxazine-3-ones Using Montmorillonite K10 under Solvent Free Conditions

  作者 KANTEVARI SRINIVAS; VUPPALAPATI SRINIVASU V N; BANTU RAJASHAKER; NAGARAPU LINGAIAH  
  选自 期刊  Journal of Heterocyclic Chemistry;  卷期  2010年47-2;  页码  313-317  
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[摘要]An efficient green protocol for the preparation of 1,2-dihydro-1-arylnaphtho[1,2-e][1,3]oxazine-3-ones employing a three-component one-pot condensation reaction of beta-naphthol, aromatic aldehyde, urea or thiourea in the presence of montmorillonite K 10 clay under solvent free conditions has been described. The present procedure offers advantages such as shorter reaction time (<90 min), simple workup, excellent yields, recovery and reusability of catalyst.

 
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