A Simple Synthesis of N-beta-Fmoc/Z-Amino Alkyl Thiols and their use in the Synthesis of N-beta-Fmoc/Z-Amino Alkyl Sulfonic Acids

[摘要]：A simple and efficient protocol for the synthesis of N-beta-Fmoc/Z-amino alkyl thiols is described. The approach uses sodium pyrosulfite-mediated hydrolysis of isothiouronium salts resulting from the reaction between N-protected aminoalkyl iodides and thiourea. N-Protected taurines were prepared through performic acid oxidation of the thiols and the products were further utilized for the synthesis of dipeptidosulfonamides.

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