- New dry arenediazonium salts, stabilized to an exceptionally high degree by the anion of o-benzenedisulfonimide
[作者:Barbero, M; Crisma, M; Degani, I; Fochi, R; Perracino, P,期刊:Synthesis, 页码:1171-1175 , 文章类型: Article,,卷期:1998年-8]
- Arenediazonium o-benzenedisulfonimides 3 (20 examples, yield > 90%) were prepared in the dry state by diazotization of aromatic amines with i-pentyl nitrite and o-benzenedisulfonimide in glacial acetic acid or formic aci...
- Palladium-catalyzed arylation and acylation of 1-benzyloxy-1,2,3-triazole through a directed ortho lithiation-transmetalation strategy
[作者:Felding, J; Uhlmann, P; Kristensen, J; Vedso, P; Begtrup, M,期刊:Synthesis, 页码:1181-1184 , 文章类型: Article,,卷期:1998年-8]
- 1-Benzyloxy-5-tributylstannyl-1,2,3-triazole was acylated with acyl chlorides in good to excellent yield using tetrakis(triphenylphosphine)palladium(0) as catalyst. Attempts to arylate failed, however 1-benzyloxy-1,2,3-t...
- Facile synthesis of novel photochromic 1,2-diheteroaryl-substituted cycloalkenes by titanium-induced intramolecular coupling reaction
[作者:Huang, ZN; Xu, BA; Jin, S; Fan, MG,期刊:Synthesis, 页码:1092-1094 , 文章类型: Article,,卷期:1998年-8]
- Intramolecular reductive coupling reaction of a series of diketones 1 and dioxo sulfides 3 induced by a low-valent titanium reagent at reflux in tetrahydrofuran affords 1,2-diheteroarylcycloalkenes 2 and 3,4-diheteroaryl...
- A new one-step synthesis of benzothiopyran derivatives
[作者:Cabiddu, MG; Cabiddu, S; Cadoni, E; Demurtas, P; Fattuoni, C; Floris, C; Melis, S,期刊:Synthesis, 页码:1098-1100 , 文章类型: Article,,卷期:1998年-8]
- (Methylthio)- and (isopropylthio)benzene are useful synthetic intermediates to prepare bimetallated intermediates which, after reaction with alpha-diketones, lead to benzothiopyranic derivatives in one-step and with good...
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