- Synthesis of Eudistomin C and E: Improved Preparation of the Indole Unit.
[作者:Yamagishi, Hiroaki;Matsumoto, Koji;Iwasaki, Kotaro;Miyazaki, Tohru;Yokoshima, Satoshi;Tokuyama, Hidetoshi;Fukuyama, Tohru;,期刊:Organic Letters, 页码:2369-2372 , 文章类型: 研究论文,,卷期:2008年10-12]
- An improved synthesis of the indole unit I, a key intermediate for eudistomin C, was established utilizing Makosza's indole synthesis. A concise total synthesis of eudistomin E (II) was achieved on the basis of the impr...
- Zinc-Catalyzed Synthesis of Pyrazolines and Pyrazoles via Hydrohydrazination.
[作者:Alex, Karolin;Tillack, Annegret;Schwarz, Nicolle;Beller, Matthias;,期刊:Organic Letters, 页码:2377-2379 , 文章类型: 研究论文,,卷期:2008年10-12]
- A novel regioselective synthesis of aryl-substituted pyrazolines I (R = H, 4-Me, 2-Cl, 4-cyano, etc.) and pyrazoles II (R = 4-Me, 2-Me, 4-i-Pr, 4-Br) has been developed. Substituted phenylhydrazines react with 3-butynol...
- Copper-Mediated Domino Process for the Synthesis of Tetraiodinated Di(perylene bisimide).
[作者:Shi, Yubai;Qian, Hualei;Li, Yan;Yue, Wan;Wang, Zhaohui;,期刊:Organic Letters, 页码:2337-2340 , 文章类型: 研究论文,,卷期:2008年10-12]
- Compounds (More Than One Hetero Atom)) Section A tetraiodinated di(perylene bisimide) was prepd. from a tetrabrominated perylene bisimide via Ullmann-type coupling, C-H transformation, and halogen-exchange. Crystal stru...
- Novel Isocyanide-Based Four-Component Reaction: A Facile Synthesis of Fully Substituted 3,4-Dihydrocoumarin Derivatives.
[作者:Shaabani, Ahmad;Soleimani, Ebrahim;Rezayan, Ali Hossein;Sarvary, Afshin;Khavasi, Hamid Reza;,期刊:Organic Letters, 页码:2581-2584 , 文章类型: 研究论文,,卷期:2008年10-12]
- A novel isocyanide-based four-component reaction between 2-hydroxybenzaldehydes, Meldrum's acid, isocyanides, and arom. or aliph. alcs. efficiently provide 3,4-dihydrocoumarin derivs., e.g. I, in good to excellent yields...
- Gold(I)-Catalyzed Divergence in the Reactivity of 3-Silyloxy 1,6-Enynes: Pinacol-Terminated vs Claisen-Terminated Cyclization Cascades.
[作者:Baskar, Baburaj;Bae, Hyo J.;An, Sang E.;Cheong, Jae Y.;Rhee, Young H.;Duschek, Alexander;Kirsch, Stefan F.;,期刊:Organic Letters, 页码:2605-2607 , 文章类型: 研究论文,,卷期:2008年10-12]
- On activation with catalytic amts. of gold(I) complexes, 3-silyloxy 1,6-enynes can react through two alternative pathways. In one, a cascade reaction consisting of carbocyclization and subsequent pinacol rearrangement t...
- Direct Synthesis of 1,3-Diketones by Rh-Catalyzed Reductive a-Acylation of Enones.
[作者:Sato, Kazuyuki;Yamazoe, Satoshi;Yamamoto, Rie;Ohata, Shizuka;Tarui, Atsushi;Omote, Masaaki;Kumadaki, Itsumaro;Ando, Akira;,期刊:Organic Letters, 页码:2405-2408 , 文章类型: 研究论文,,卷期:2008年10-12]
- 1,3-Diketones were synthesized from a,b-unsatd. ketones by treatment with acid chlorides and Et2Zn in the presence of RhCl(PPh3)3. Thus, reaction of MeCOCH:CH2 with PhCOCl in THF contg. RhCl(PPh3)3 and Et2Zn at 0?to roo...
- Efficient Preparation of Terminal Conjugated Dienes by Coupling of Dienol Phosphates with Grignard Reagents under Iron Catalysis.
[作者:Cahiez, Gerard;Habiak, Vanessa;Gager, Olivier;,期刊:Organic Letters, 页码:2389-2392 , 文章类型: 研究论文,,卷期:2008年10-12]
- An efficient new route to prep. stereoselectively terminal conjugated dienes, e.g. (E)-n-C8H17CH:CHCH:CH2, by coupling Grignard reagents and dienol phosphates, e.g. (E)-H2C:CHCH:CHOPO(OEt)2, in the presence of Fe(acac)3 ...
- Alcohol Uncaging with Fluorescence Reporting: Evaluation of o-Acetoxyphenyl Methyloxazolone Precursors.
[作者:Gagey, Nathalie;Emond, Matthieu;Neveu, Pierre;Benbrahim, Chouaha;Goetz, Bernard;Aujard, Isabelle;Baudin, Jean-Bernard;Jullien, Ludovic;,期刊:Organic Letters, 页码:2341-2344 , 文章类型: 研究论文,,卷期:2008年10-12]
- This paper evaluates a series of photolabile protecting groups with built-in fluorescence reporting. They rely on readily available o-acetoxyphenyl methyloxazolones as activated precursors. Alc. substrates are easily c...
- N-Heterocyclic Carbene (NHC)-Catalyzed Direct Amidation of Aldehydes with Nitroso Compounds.
[作者:Wong, Fong Tian;Patra, Pranab K.;Seayad, Jayasree;Zhang, Yugen;Ying, Jackie Y.;,期刊:Organic Letters, 页码:2333-2336 , 文章类型: 研究论文,,卷期:2008年10-12]
- N-Heterocyclic carbene-catalyzed direct amidation of aldehydes R1CHO (R1 = H2C:CH, cyclopropyl, Bu, EtO2CCH:CH, Ph, cyclohexyl, 4-MeOC6H4, etc.) with nitrosoarenes R2NO (R2 = Ph, 2-MeC6H4, 2,6-F2C6H3, 4-Me2NC6H4, 3,5-Me2...
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