- Recent Mechanistic Insights in the Singlet Oxygen Ene Reaction
[作者:ALBERTI MARIZA N; ORFANOPOULOS MICHAEL,期刊:SYNLETT, 页码:999-1026 , 文章类型: Article,,卷期:2010年-7]
- Singlet oxygen reacts with alkenes, which bear allylic hydrogens, in an ene fashion to afford allylic hydroperoxides. This reaction, apart from its synthetic usefulness, has received extensive mechanistic attention. Nume...
- Intramolecular Cobalt-Catalyzed [2+2+2] Cycloaddition of O-Protected Diyne-Cyanohydrins
[作者:MEISSNER ANJA; GROTH ULRICH,期刊:SYNLETT, 页码:1051-1054 , 文章类型: Article,,卷期:2010年-7]
- O-Protected cyanohydrins were found to serve as a source of the nitrile within the intramolecular cobalt-mediated [2+2+2] cycloaddition to pyridines. Several 6-substituted 1,2,3,4,7,8,9,10-octahydrophenanthridines were s...
- Synthesis of a Deoxyxylopuromycin Analogue
[作者:KRISHNAKUMAR KOLLAPPILLIL S; STRAZEWSKI PETER,期刊:SYNLETT, 页码:1055-1058 , 文章类型: Article,,卷期:2010年-7]
- N-6-Bis-demethylated deoxyxylopuromycin was synthesized over six steps in 56% overall yield. The key steps are Mitsunobu reaction with DPPA and a Staudinger-Vilarrasa coupling.
- Isoxazolopyrimidines as Novel Delta F508-CFTR Correctors
[作者:YU GUI JUN; YANG BAOXUE; VERKMAN A S; KURTH MARK J,期刊:SYNLETT, 页码:1063-1066 , 文章类型: Article,,卷期:2010年-7]
- Using a cell-based high-throughput screen, we identified isoxazolo[5,4-d]pyrimidines as novel small-molecule correctors of the cystic fibrosis mutant protein Delta F508-CFTR. 22 Isoxazolo[5,4-d] pyrimidine analogues were...
- Microwave-Assisted Preparation of Quinolone and Quinoline Derivatives
[作者:ALBRECHT MARKUS; OSETSKA OLGA; RANTANEN TONI; FROEHLICH ROLAND; BOLMA CARSTEN,期刊:SYNLETT, 页码:1081-1084 , 文章类型: Article,,卷期:2010年-7]
- Quinolinone derivatives can be obtained in microwaveassisted syntheses by reaction of aniline derivatives with acetylene dicarboxylic esters, a malonic acid diester or beta-keto ester derivatives. The reaction proceeds u...
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