- Convenient Chlorination with Concentrated Hydrochloric Acid in the Presence of Iodosylbenzene
[作者:KITAMURA TSUGIO; TAZAWA YUI; MORSHED MOHAMMAD HASAN; KOBAYASHI SOICHI,期刊:Synthesis, 页码:1159-1162 , 文章类型: Article,,卷期:2012年44-8]
- An efficient chlorination of beta-keto esters, 1,3-diketones, and alkenes was performed conveniently with concentrated HCl in the presence of PhIO, selectively giving alpha-chloro-beta-keto esters, 2-chloro-1,3-diketones...
- Synthesis of Phloroglucinol Monoaryl Ethers
[作者:SHERWOOD ALEXANDER M; POND DAVID M; TRUDELL MARK L,期刊:Synthesis, 页码:1208-1212 , 文章类型: Article,,卷期:2012年44-8]
- A variety of novel functionalized phloroglucinol monoaryl ethers have been synthesized using a two-step procedure. Target ethers were synthesized by coupling electron-deficient aryl fluorides with 3,5-dimethoxyphenol via...
- Synthesis of Aryl Triolborates via Nickel-Catalyzed Borylation of Aryl Halides with 5-(tert-Butyldimethylsiloxymethyl)-5-methyl-1,3,2-dioxaborinane
[作者:SOGABE YOSUKE; NAMIKOSHI TAKESHI; WATANABE SHINJI; MURATA MIKI,期刊:Synthesis, 页码:1233-1236 , 文章类型: Article,,卷期:2012年44-8]
- The nickel-catalyzed borylation of aryl halides with 5-(tert-butyldimethylsiloxymethyl)-5-methyl-1,3,2-dioxaborinane, prepared in situ, was achieved. The mild reaction conditions allowed common functional groups in the a...
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